Carbon number | δc | δH, coupling pattern, J in Hz | ||||||
---|---|---|---|---|---|---|---|---|
1 | 2 | 3 | 4 | 1 | 2 | 3 | 4 | |
2 | 147.59 | 148.06 | 158.54 | 158.99 | Â | Â | Â | Â |
3 | 137.70 | 137.27 | 135.47 | 135.63 | Â | Â | Â | Â |
4 | 177.12 | 177.45 | 179.51 | 179.42 | Â | Â | Â | Â |
5 | 162.28 | 162.53 | 162.80 | 162.97 | Â | Â | Â | Â |
6 | 99.09 | 99.28 | 99.96 | 99.89 | 6.73, br. s | 6.16, d, 2.0 | 6.19, d, 2.0 | 6.17, br. s |
7 | 165.37 | 165.92 | 166.13 | 165.96 | Â | Â | Â | Â |
8 | 94.16 | 94.45 | 94.80 | 94.72 | 6.68, br, s | 6.36, d, 2.0 | 6.39, d, 2.0 | 6.36, br. s |
9 | 157.33 | 158.26 | 159.08 | 158.39 | Â | Â | Â | Â |
10 | 104.31 | 104.54 | 104.09 | 105.48 | Â | Â | Â | Â |
1′ | 123.43 | 123.76 | 122.80 | 122.92 |  |  |  |  |
2′ | 116.48 | 130.66 | 132.28 | 117.58 | 8.55, br. s | 8.07, d, 9.2 | 8.05, d, 8.8 | 7.70, d, 2.0 |
3′ | 149.66 | 116.30 | 116.08 | 145.84 |  | 6.89, d, 9.2 | 6.88, d, 9.2 |  |
4′ | 146.91 | 160.54 | 161.58 | 149.82 |  |  |  |  |
5′ | 116.48 | 116.30 | 116.08 | 115.98 | 7.35, d, 8.4 | 6.89, d, 9.2 | 6.88, d, 9.2 | 6.85, d, 8.4 |
6′ | 120.93 | 130.66 | 132.28 | 123.19 | 8.08, br. d, 8.4 | 8.07, d, 9.2 | 8.05, d, 8.8 | 7.56, dd, 8.4, 2.0 |
1″ |  |  | 104.09 | 104.41 |  |  | 5.24, d, 7.2 | 5.22, d, 7.2 |
2″ |  |  | 75.74 | 75.70 |  |  |  |  |
3″ |  |  | 78.43 | 78.32 |  |  |  |  |
4″ |  |  | 71.37 | 71.17 |  |  |  |  |
5″ |  |  | 78.05 | 78.08 |  |  |  |  |
6″ |  |  | 62.64 | 62.53 |  |  | 3.68, dd, 12.0, 2.4 3.52, dd, 12.0, 5.2 | 3.71, dd, 12.0, 2.4 3.58, dd, 12.0, 5.2 |