Fig. 4From: Nuclear magnetic resonance assignment strategy for pentacyclic triterpenes, using lup-20(29)-ene from Pilotrichella flexilis as model system, combining spectrally filtered proton-to-carbon schemes and DFT–GIAO approachTwo-dimensional 1H–1H homonuclear correlation spectrum via dipolar coupling (EXSY) of lup-20(29)-ene, with 1.4 s of mixing time. Key inter-nuclear correlations between resonances involving methyls are shown in the spectrum, as well as in the molecular formulaBack to article page