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Table 1 NMR data for butyroscavin (1)

From: Butenolide derivatives from the fungus Aspergillus terreus and their radical scavenging activity and protective activity against glutamate-induced excitotoxicity

Position

Butyroscavin (1)

 

13Ca

1H (mult.)a

HMBC

1

169.6

  

2

138.6

  

3

128.0

  

4

85.7

  

5

38.3

3.42 (2H, s)

C-4, C-1″, C-2″

6

169.8

  

7

62.5

4.25 (2H, q, J = 7.2 Hz)

C-8, C-6

8

13.0

1.21 (3H, t, J = 7.2 Hz)

C-7

1′

121.9

  

2′

129.2

7.60 (2H, d, J = 8.8 Hz)

C-3, C-2′, C-4′

3′

115.4

6.87 (2H, d, J = 8.8 Hz)

C-1′, C-3′, C-4′

4′

158.2

  

1″

124.1

  

2″

131.3

6.64 (2H, d, J = 8.8 Hz)

C-5, C-2″, C-4″

3″

114.4

6.51 (2H, d, J = 8.8 Hz)

C-1″, C-3″, c C-4″

4″

156.3

  
  1. a 1H and 13C NMR were measured at 400 MHz and 100 MHz, respectively, in CD3OD and solvent signals were used as reference