EfPhoP-RD | ||
---|---|---|
Thick plate-shape | Thin rod-shape | |
Diffraction source | Beamline 7A, PAL | |
Wavelength (Å) | 1.0000 | |
Detector | ADSC Quantum 270r CCD | |
Crystal-to-detector distance (mm) | 450 | 350 |
Rotation range per image (°) | 1 | 1 |
Total rotation range (°) | 180 | 360 |
Exposure time per image (s) | 5 | 2 |
Space group | P212121 | C2221 |
Unit-cell parameters (Å, °) | a = 188.63, b = 187.71, c = 197.49 α = β = γ = 90 | a = 118.74, b = 189.83, c = 189.88 α = β = γ = 90 |
Resolution range (Å) | 50.0−5.0 (5.18−5.00) | 50.0−3.5 (3.63−3.50) |
Total no. of reflections | 628,425 | 1,931,024 |
No. of unique reflections | 26,755 | 20,764 |
Completeness (%) | 87.1 (81.2) | 75.4 (65.1) |
Multiplicity | 3.0 (1.9) | 2.5 (1.7) |
<I/σ(I)> | 10.8 (2.0) | 6.6 (2.4) |
CC1/2 | 0.994 (0.172) | 0.973 (0.334) |
Ramerge (%) | 10.1 (35.1) | 14.3 (34.9) |