Table 3 Reproducibility relative standard deviation (RSDR; n = 6), repeatability relative standard deviation (RSDr; n = 6), recoveries, linear range, LOD, LOQ and coefficient of estimation (r2)a
Target compound | Linear range (µg/L) | Limit of detection (LOD) (µg/L) | Limit of quantification (LOQ) (µg/L) | Coefficient of estimation (r2) | Recoveries (%) | Repeatability (RSDr) (%) | Reproducibility (RSDR) (%) |
|---|---|---|---|---|---|---|---|
Na | 0.005–10 | 0.01 | 0.03 | 0.995 | 95.3 | 7.8 | 7, 11, 13 |
Ace | 0.005–10 | 0.04 | 0.12 | 0.991 | 96.4 | 9.5 | 8, 10, 18 |
Ac | 0.005–10 | 0.03 | 0.08 | 0.984 | 100.2 | 5.3 | 7, 9,14 |
F | 0.005–10 | 0.06 | 0.20 | 0.989 | 92.5 | 4.6 | 6, 9, 10 |
Ph | 0.005–10 | 0.02 | 0.06 | 0.993 | 98.1 | 7.7 | 11, 13, 15 |
A | 0.005–10 | 0.02 | 0.07 | 0.996 | 103.4 | 10.2 | 8, 11, 14 |
Fl | 0.005–10 | 0.05 | 0.18 | 0.990 | 101.6 | 7.8 | 8, 10, 16 |
P | 0.005–10 | 0.02 | 0.07 | 0.986 | 98.7 | 8.3 | 11, 13, 17 |
B(a)A | 0.005–10 | 0.10 | 0.32 | 0.984 | 99.2 | 6.6 | 10, 12, 14 |
Ch | 0.005–10 | 0.19 | 0.64 | 0.994 | 101.4 | 8.6 | 7, 10, 15 |
B(b)F | 0.005–10 | 0.13 | 0.43 | 0.996 | 98.8 | 9.3 | 9, 11, 16 |
B(k)F | 0.005–10 | 0.11 | 0.35 | 0.989 | 99.2 | 6.9 | 7, 10, 14 |
B(a)P | 0.005–10 | 0.15 | 0.50 | 0.987 | 99.1 | 9.5 | 11, 13, 17 |
D(h)A | 0.005–10 | 0.14 | 0.46 | 0.995 | 100.3 | 10 | 9, 12, 18 |
B(g)P | 0.005–10 | 0.21 | 0.70 | 0.994 | 102.4 | 9.9 | 10, 13, 15 |
I(cd)P | 0.005–10 | 0.09 | 0.30 | 0.990 | 101.3 | 9.6 | 11, 14, 17 |