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Table 2 The extraction efficiency of seven metabolites according to the ratio of acetonitrile (ACN) and water mixture in soybean

From: Development of simultaneous analytical method for the determination of fluazaindolizine and its seven metabolites in agricultural products by liquid chromatography tandem mass spectrometry

Compound

Recovery ± SDa (%)

ACN: water (70:30)

ACN: water (80:20)

ACN: water (90:10)

ACN: water (100:0)

IN-A5760

76.1 ± 3.6

92.4 ± 9.3

89.1 ± 7.3

91.3 ± 0.2

IN-F4106

93.1 ± 2.9

95.3 ± 6.1

96.7 ± 3.8

95.4 ± 2.4

IN-QEK31

88.6 ± 0.9

85.3 ± 2.8

87.1 ± 1.2

89.3 ± 2.2

IN-QZY47

85.6 ± 3.3

99.1 ± 6.2

81.4 ± 4.4

76.2 ± 5.0

IN-TMQ01

88.0 ± 1.5

91.0 ± 0.4

88.7 ± 0.2

88.2 ± 2.0

IN-UNS90

80.0 ± 1.9

84.0 ± 1.4

82.2 ± 3.2

84.1 ± 2.9

IN-UJV12

65.0 ± 3.4

46.0 ± 0.5

42.2 ± 4.3

26.9 ± 0.5

  1. aMean values of 3 times repetitions with standard deviation