Skip to main content

Table 5 Recovery results of fluazaindolizine and seven metabolites in five agricultural products

From: Development of simultaneous analytical method for the determination of fluazaindolizine and its seven metabolites in agricultural products by liquid chromatography tandem mass spectrometry

Sample

Fortification levels (mg/kg)

Recovery ± CVa (%)

Fluazaindolizine

IN-A5760

IN-F4106

IN-QEK31

IN-QZY47

IN-TMQ01

IN-UNS90

IN-UJV12

Hulled rice

0.01 (0.05)

109.5 ± 3.1

97.7 ± 6.0

88.1 ± 4.9

91.1 ± 1.4

101.0 ± 3.0

85.4 ± 4.4

84.3 ± 3.5

87.0 ± 2.0

0.1 (0.5)

86.7 ± 2.3

94.0 ± 2.0

99.1 ± 5.4

94.9 ± 1.7

89.8 ± 3.0

93.3 ± 0.9

87.0 ± 2.6

90.0 ± 2.2

0.5 (2.5)

86.1 ± 3.1

90.5 ± 1.8

94.8 ± 2.4

93.5 ± 1.1

86.0 ± 1.4

89.4 ± 2.5

86.8 ± 2.8

88.9 ± 1.6

Potato

0.01 (0.05)

104.3 ± 3.0

94.8 ± 3.8

89.7 ± 5.0

99.4 ± 2.4

86.5 ± 3.8

98.2 ± 3.0

95.1 ± 4.2

89.0 ± 3.7

0.1 (0.5)

99.1 ± 1.7

95.6 ± 2.5

89.1 ± 4.4

98.7 ± 1.6

85.5 ± 2.9

107.4 ± 2.9

110.0 ± 2.6

88.4 ± 2.0

0.5 (2.5)

99.9 ± 2.2

93.9 ± 1.6

89.1 ± 3.4

97.6 ± 0.2

83.7 ± 1.1

105.5 ± 1.3

109.8 ± 1.4

89.1 ± 3.1

Soybean

0.01 (0.05)

89.3 ± 2.3

106.1 ± 4.7

88.9 ± 9.1

92.6 ± 3.5

91.7 ± 1.9

91.5 ± 6.0

85.9 ± 2.2

91.4 ± 3.5

0.1 (0.5)

81.8 ± 5.7

82.6 ± 3.9

87.8 ± 2.8

85.6 ± 2.0

82.6 ± 2.3

82.4 ± 2.5

85.8 ± 0.9

78.9 ± 1.4

0.5 (2.5)

83.5 ± 5.5

80.6 ± 3.8

87.7 ± 4.1

85.6 ± 3.5

79.0 ± 1.8

83.9 ± 2.6

85.1 ± 1.2

76.5 ± 2.0

Mandarin

0.01 (0.05)

94.5 ± 2.9

93.9 ± 2.2

86.7 ± 8.8

94.1 ± 0.8

95.1 ± 5.6

91.6 ± 3.0

91.0 ± 2.3

96.3 ± 6.2

0.1 (0.5)

95.3 ± 3.0

97.8 ± 3.6

89.1 ± 4.7

96.4 ± 1.5

93.6 ± 1.6

90.0 ± 2.0

95.0 ± 1.4

101.6 ± 1.0

0.5 (2.5)

95.0 ± 1.8

95.2 ± 2.9

86.5 ± 3.8

96.8 ± 2.2

92.1 ± 1.1

90.4 ± 2.7

95.1 ± 1.5

97.0 ± 2.0

Green pepper

0.01 (0.05)

93.5 ± 2.6

96.7 ± 6.4

88.4 ± 4.5

86.4 ± 4.3

89.7 ± 2.0

92.0 ± 6.0

86.6 ± 1.5

102.2 ± 3.8

0.1 (0.5)

97.4 ± 1.7

89.0 ± 1.9

88.0 ± 2.1

91.7 ± 1.1

89.5 ± 1.1

93.5 ± 1.2

92.7 ± 2.7

97.8 ± 1.5

0.5 (2.5)

98.9 ± 2.8

89.9 ± 4.3

86.8 ± 6.0

90.3 ± 1.5

88.9 ± 3.8

91.3 ± 3.2

92.8 ± 5.2

96.3 ± 2.9

  1. aMean values of 5 times repetitions with coefficient of variation
  2. Note: (*) was the fortification levels for IN-A5760, IN-F4106, IN-QZY47 and IN-UJV1