Compound 1 | 13 C [23] | ||
---|---|---|---|
Position | 1H | 13C | |
1 | 37.3 | 37.2 | |
2 | 31.6 | 31.6 | |
3 | 3.51 (m, 1 H) | 71.9 | 71.8 |
4 | 2.33 (m, 1 H) | 42.2 | 42.3 |
5 | 140.8 | 140.7 | |
6 | 5.33 (m, 1 H) | 121.8 | 121.7 |
7 | 2.00 (d, J = 7.0 Hz, 2 H) | 32.0 | 31.9 |
8 | 32.0 | 31.9 | |
9 | 50.2 | 50.1 | |
10 | 36.6 | 36.5 | |
11 | 22.8 | 21.1 | |
12 | 39.8 | 39.8 | |
13 | 42.4 | 42.3 | |
14 | 56.8 | 56.7 | |
15 | 24.4 | 24.3 | |
16 | 28.3 | 28.2 | |
17 | 56.1 | 56.0 | |
18 | 0.67 (s, 3 H) | 11.9 | 11.8 |
19 | 0.99 (s, 3 H) | 19.1 | 19.4 |
20 | 36.2 | 36.1 | |
21 | 0.87 (d, J = 6.9 Hz, 3 H) | 18.8 | 18.8 |
22 | 34.1 | 33.9 | |
23 | 26.1 | 26.1 | |
24 | 45.9 | 45.8 | |
25 | 29.2 | 29.1 | |
26 | 0.85 (d, J = 6.9 Hz, 3 H) | 19.9 | 19.8 |
27 | 0.81 (d, J = 7.2 Hz, 3 H) | 19.5 | 19.0 |
28 | 23.1 | 23.1 | |
29 | 0.76 (m, 3 H) | 12.1 | 12.0 |