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Table 1 LC–MS method precision (RSD, %) and accuracy (recovery, %) for catechin and epicatechin using SIL-IS

From: Improved quantification of catechin and epicatechin in red rice (Oryza sativa L.) using stable isotope dilution liquid chromatography-mass spectrometry

Concentration (μg/mL)

Precision (RSD, %)

Accuracy (Recovery, %)

Catechina

Epicatechinb

Catechina

Epicatechinb

5

1.53

0.53

99.67 ± 1.52

99.40 ± 0.52

2.5

2.17

1.30

101.48 ± 2.20

102.24 ± 1.33

1.25

1.29

1.71

99.82 ± 1.29

101.11 ± 1.73

0.63

2.62

3.17

99.83 ± 2.61

100.43 ± 3.18

  1. aCatechin-2,3,4-13C3
  2. bepicatechin-2,3,4-13C3
  3. SIL-IS stable-isotope-labeled internal standard