Fig. 3From: Nuclear magnetic resonance assignment strategy for pentacyclic triterpenes, using lup-20(29)-ene from Pilotrichella flexilis as model system, combining spectrally filtered proton-to-carbon schemes and DFT–GIAO approachTwo-dimensional 1H–13C HMBC correlation spectra of lup-20(29)-ene promoting; top: long range heteronuclear coupling contacts of around 2 Hz (d6 = 250 ms) and bottom: promotion of 3, 4, 5JH–X short-to long range heteronuclear contacts of around 7 Hz (d6 = 62.5 ms as the standard condition)Back to article page