Table 3 Bond angles (°) of endosulfan sulfate
Bond | A-1 | A-2 | B |
|---|---|---|---|
C(8)–O(1)–S(1) | 118.42(15) | 118.90(16) | 117.89(14) |
C(9)–O(2)–S(1) | 119.23(15) | 118.37(15) | 117.63(14) |
O(4)–S(1)–O(3) | 120.26(11) | 121.54(12) | 120.97(12) |
O(4)–S(1)–O(2) | 106.41(11) | 106.54(12) | 109.88(10) |
O(3)–S(1)–O(2) | 110.06(11) | 109.33(10) | 106.09(12) |
O(4)–S(1)–O(1) | 105.95(12) | 104.84(11) | 108.93(11) |
O(3)–S(1)–O(1) | 109.49(11) | 110.10(12) | 105.91(11) |
O(2)–S(1)–O(1) | 103.31(9) | 102.86(9) | 103.61(9) |
C(6)–C(1)–C(2) | 107.32(17) | 107.11(19) | 108.08(16) |
C(6)–C(1)–Cl(1) | 127.83(17) | 128.07(18) | 128.21(16) |
C(2)–C(1)–Cl(1) | 124.83(15) | 124.80(16) | 123.54(16) |
C(1)–C(2)–C(7) | 98.74(16) | 98.49(18) | 98.84(15) |
C(1)–C(2)–C(3) | 109.53(16) | 109.78(17) | 108.24(16) |
C(7)–C(2)–C(3) | 101.07(15) | 100.93(18) | 100.85(14) |
C(1)–C(2)–Cl(2) | 116.10(14) | 115.83(16) | 115.66(14) |
C(7)–C(2)–Cl(2) | 116.14(14) | 116.37(16) | 116.04(14) |
C(3)–C(2)–Cl(2) | 113.41(14) | 113.56(16) | 115.10(13) |
C(8)–C(3)–C(4) | 119.87(18) | 118.40(19) | 117.55(17) |
C(8)–C(3)–C(2) | 115.06(18) | 116.8(2) | 111.97(16) |
C(4)–C(3)–C(2) | 102.62(15) | 102.66(17) | 102.60(15) |
C(9)–C(4)–C(3) | 118.44(18) | 118.55(18) | 117.36(17) |
C(9)–C(4)–C(5) | 115.66(18) | 115.51(19) | 111.52(16) |
C(3)–C(4)–C(5) | 102.85(16) | 102.32(17) | 102.41(15) |
C(6)–C(5)–C(7) | 98.64(16) | 98.62(17) | 99.60(16) |
C(6)–C(5)–C(4) | 108.76(16) | 108.43(17) | 107.70(15) |
C(7)–C(5)–C(4) | 101.00(17) | 101.74(17) | 101.55(15) |
C(6)–C(5)–Cl(5) | 116.10(16) | 116.37(16) | 115.46(14) |
C(7)–C(5)–Cl(5) | 115.93(14) | 116.09(16) | 116.31(14) |
C(4)–C(5)–Cl(5) | 114.37(14) | 113.68(15) | 114.33(14) |
C(1)–C(6)–C(5) | 107.78(18) | 107.99(18) | 107.08(17) |
C(1)–C(6)–Cl(6) | 128.12(17) | 128.07(18) | 129.01(16) |
C(5)–C(6)–Cl(6) | 124.08(16) | 123.80(16) | 123.74(16) |
C(2)–C(7)–C(5) | 92.04(15) | 92.23(16) | 92.47(14) |
C(2)–C(7)–Cl(4) | 114.38(15) | 114.81(17) | 114.26(13) |
C(5)–C(7)–Cl(4) | 114.52(15) | 113.88(17) | 113.97(14) |
C(2)–C(7)–Cl(3) | 113.95(14) | 113.91(18) | 113.96(13) |
C(5)–C(7)–Cl(3) | 113.94(15) | 113.77(17) | 113.49(13) |
Cl(4)–C(7)–Cl(3) | 107.64(11) | 107.84(13) | 108.23(11) |
O(1)–C(8)–C(3) | 114.19(17) | 113.50(19) | 109.12(17) |
O(2)–C(9)–C(4) | 113.86(17) | 113.70(17) | 108.94(17) |