No | δCa | δH (J, Hz)b | HMBC |
---|---|---|---|
1 | 34.6 | 1.33 (1H, m) 2.06 (1H, dd, J = 13.6, 4.4 Hz) | C2, C10, C14 |
2 | 22.3 | 1.60 (2H, m) | Â |
3 | 36.3 | 1.96 (1H, m) 2.35 (1H, m) | C2, C4, C15 C4 |
4 | 148.9 | Â | Â |
5 | 42.2 | 2.38 (1H, m) | C10 |
6 | 25.6 | 2.31 (1H, m) 2.67 (1H, dq, J = 12.8, 2.8 Hz) | C7, C10 C7, C8, C10 |
7 | 159.1 | Â | Â |
8 | 79.9 | 4.98 (1H, d, J = 2.0 Hz) |  |
9 | 75.4 | 3.88 (1H, d, J = 3.6 Hz) | C5, C7, C8 |
10 | 41.0 | Â | Â |
11 | 121.9 | Â | Â |
12 | 175.1 | Â | Â |
13 | 8.4 | 1.83 (3H, t, J = 1.6 Hz) | C7, C11, C12 |
14 | 15.7 | 0.89 (3H, s) | C1, C5, C9, C10 |
15 | 107.3 | 4.88 (1H, d, J = 1.6 Hz) 4.60 (1H, d, J = 1.6 Hz) | C3, C5 |